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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List (4-isopropoxyphenyl)methanamine hydrochloride
100131-60-0

(4-isopropoxyphenyl)methanamine hydrochloride synthesis

1synthesis methods
(E)-N-{[4-(propan-2-yloxy)phenyl]methylidene}hydroxylamine

91342-00-6
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(4-isopropoxyphenyl)methanamine hydrochloride

100131-60-0
20 suppliers
$45.00/5mg

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Yield:100131-60-0 70%

Reaction Conditions:

Stage #1: 4-Isopropyloxy-benzaldoximwith lithium aluminium tetrahydride in tetrahydrofuran at 20; for 4 h;Reflux;
Stage #2: with hydrogenchloride in 1,4-dioxane;ethyl acetate;

References:

Musatov;Starodubtseva;Turova;Kurilov;Vinogradov;Rakishev;Struchkova [Russian Journal of Organic Chemistry,2010,vol. 46,# 7,p. 1021 - 1028] Location in patent:experimental part