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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 4-Methoxy-3,5-diMethylpicolinonitrile
104916-41-8

4-Methoxy-3,5-diMethylpicolinonitrile synthesis

6synthesis methods
187222-12-4 Synthesis
4H-Pyran-2-carboxylic acid, 3,5-dimethyl-4-oxo-

187222-12-4
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4-Methoxy-3,5-diMethylpicolinonitrile

104916-41-8
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-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 92 percent / sulfuric acid / 4 h / Heating
2: 91 percent / ammonia / ethanol / 48 h / 120 °C
3: 90 percent / anh. potassium carbonate / acetone / 15 h / Heating
4: 91 percent / pyridine, trifluoroacetic anhydride / CH2Cl2 / Ambient temperature

References:

Chou, Shan-Yen;Chen, Shyh-Fong [Heterocycles,1997,vol. 45,# 1,p. 77 - 85]

1-Penten-3-one, 1-hydroxy-2-methyl-

50421-81-3
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4-Methoxy-3,5-diMethylpicolinonitrile

104916-41-8
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References
2-Pyridinecarboxamide, 1,4-dihydro-3,5-dimethyl-4-oxo-

187222-20-4
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4-Methoxy-3,5-diMethylpicolinonitrile

104916-41-8
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References
3,5-DiMethyl-2-(ethoxycarbonyl)-4-pyrone

187222-13-5
12 suppliers
$165.00/100mg

4-Methoxy-3,5-diMethylpicolinonitrile

104916-41-8
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References
4-methoxy-3,5-dimethylpicolinaldehyde

110464-72-7
54 suppliers
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4-Methoxy-3,5-diMethylpicolinonitrile

104916-41-8
14 suppliers
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References