(4-methylisoxazol-5-yl)methanol synthesis

1synthesis methods

Product Name:(4-methylisoxazol-5-yl)methanol
CAS Number:1607024-83-8
Molecular formula:C5H7NO2
Molecular Weight:113.11

121781-57-5 Synthesis

(E)-1,1,1-trichloro-4-ethoxy-3-methylbut-3-en-2-one

121781-57-5
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1607024-83-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sulfuric acid / ethanol / 85 °C
2: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

References:

WO2014/66795,2014,A1

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