4-methyloctan-1-ol synthesis
- Product Name:4-methyloctan-1-ol
- CAS Number:38514-03-3
- Molecular formula:C9H20O
- Molecular Weight:144.2545
4536-23-6
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: 8.04 g / LiAlH4 / diethyl ether / 20 °C
2.1: 11.2 g / red phosphorus; bromine / 0 - 20 °C
3.1: NaOEt / ethanol / 0.12 h / Heating
3.2: ethanol / 1 h / Heating
4.1: KOH / ethanol / 4 h / Heating
5.1: 3 h / 190 °C
6.1: 2.00 g / LiAlH4 / diethyl ether / 20 °C
References:
Hedenstroem, Erik;Nguyen, Ba-Vu;Silks III, Louis A. [Tetrahedron Asymmetry,2002,vol. 13,# 8,p. 835 - 844]
56196-53-3
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54947-74-9
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1000210-73-0
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