Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
logo
Inquriy
Try our best to find the right business for you.
Messages
Do not miss inquiry messages Please log in to view all inquiry messages.
My chemicalbook

Welcome back!

Structured search
18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List (4-METHYLPYRIDIN-3-YL)METHYLAMINE
1443-42-1

(4-METHYLPYRIDIN-3-YL)METHYLAMINE synthesis

3synthesis methods
4-Methyl-3-pyridinecarboxamide

7250-52-4
74 suppliers
$32.00/100mg

(4-METHYLPYRIDIN-3-YL)METHYLAMINE

1443-42-1
56 suppliers
$57.00/100mg

-

Yield: 95%

Reaction Conditions:

with dimethylsulfide borane complex in tetrahydrofuran at 0 - 20;

Steps:

13
Example 13: Synthesis of 3-aminomethyl-4-methylpyridine EPO 100106] A round bottom flask was charged with 0.45g (3.3OmM) of 4- methylnicotinamide (27). The flask was flushed with argon, and 5OmL of dry THF was added by syringe. The resulting solution was cooled to 0 dg C, and 2.5mL (4.96mM) of a 2M solution of borane-dimethylsulfde complex (in THF) was added. A bubbler was attached, and the solution was allowed to warm to RT overnight. The solution was quenched with MeOH, and dried and evaporated to give 0.38g (95%) of 3-aminomethyl- 4-methylpyridine (28).

References:

PHARMACOPEIA DRUG DISCOVERY, INC. WO2006/108103, 2006, A1 Location in patent:Page/Page column 32-33

3-Cyano-4-methylpyridine

5444-01-9
229 suppliers
$16.00/1 g

(4-METHYLPYRIDIN-3-YL)METHYLAMINE

1443-42-1
56 suppliers
$57.00/100mg

References
4-Methylnicotinic acid

3222-50-2
195 suppliers
$12.72/500mgs:

(4-METHYLPYRIDIN-3-YL)METHYLAMINE

1443-42-1
56 suppliers
$57.00/100mg

References

(4-METHYLPYRIDIN-3-YL)METHYLAMINE Related Search:

4-(TRIFLUOROMETHYL)PYRIDINE-3-CARBOXYLIC ACID HYDRAZIDE 3,4-PYRIDINEDICARBOXIMIDE 2,5-DICHLORO-4,6-DIMETHYLNICOTINAMIDE