[4-(Methylthio)phenyl]-hydrazinehydrochloride synthesis
- Product Name:[4-(Methylthio)phenyl]-hydrazinehydrochloride
- CAS Number:58626-97-4
- Molecular formula:C7H11ClN2S
- Molecular Weight:190.6936
104-95-0
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$8.00/5g
58626-97-4
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Yield:58626-97-4 87%
Reaction Conditions:
Stage #1: (4-bromophenyl)thioanisolewith potassium phosphate;copper(l) iodide;N,N′-bis(2,6-dimethylphenyl)oxalamide;cetyltrimethylammonim bromide in water at 80; for 0.25 h;Schlenk technique;Inert atmosphere;Sealed tube;
Stage #2: with hydrazine hydrate in water at 80;Inert atmosphere;Schlenk technique;Sealed tube;
Stage #3: with hydrogenchloride in water; pH=3 - 4;Inert atmosphere;Schlenk technique;Sealed tube;
References:
Kumar, Siripuram Vijay;Ma, Dawei [Chinese Journal of Chemistry,2018,vol. 36,# 11,p. 1003 - 1006] Location in patent:supporting information
104-96-1
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58626-97-4
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115171-09-0
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58626-97-4
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18620-04-7
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$187.00/50mL
58626-97-4
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