4'-Octyl[1,1'-biphenyl]-4-carbonitrile synthesis
- Product Name:4'-Octyl[1,1'-biphenyl]-4-carbonitrile
- CAS Number:52709-84-9
- Molecular formula:C21H25N
- Molecular Weight:291.43
92-52-4
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52709-84-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 83 percent / acetic anhydride / 2 h / Heating
References:
Ruolene, Yu. I.;Adomenas, P. V.;Sirutkaitis, R. A.;Denis, G. I. [Journal of Organic Chemistry USSR (English Translation),1984,vol. 20,p. 1187 - 1191][Zhurnal Organicheskoi Khimii,1984,vol. 20,# 6,p. 1305 - 1310]
![[1,1'-Biphenyl]-4-carboxaldehyde, 4'-octyl-, oxime](/CAS/20210305/GIF/93972-16-8.gif)
93972-16-8
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52709-84-9
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111-64-8
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$15.00/25mL
52709-84-9
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71691-02-6
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47162-00-5
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52709-84-9
141 suppliers
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