4-PIPERAZIN-1-YL-BENZOIC ACID synthesis
- Product Name:4-PIPERAZIN-1-YL-BENZOIC ACID
- CAS Number:85474-75-5
- Molecular formula:C11H14N2O2
- Molecular Weight:206.24
162046-66-4
146 suppliers
$6.00/250mg
85474-75-5
81 suppliers
$86.00/250mg
Yield:85474-75-5 61%
Reaction Conditions:
in hydrogenchloride;methanol;
Steps:
7.a (a)
(a) 4-piperazin-1-yl-benzoic acid A mixture of 4-(4-(tert-butoxycarbonyl)piperazin-1-yl)benzoic acid (28 g, 91 mmol) in hydrochloric acid in methanol (300 mL) was stirred at room temperature for 4 h. The resulting precipitate was collected by filtration and concentrated to dryness to provide the title compound (17 g, 61% yield) as a white solid.
References:
US2012/114600,2012,A1
451-46-7
282 suppliers
$5.00/5g
85474-75-5
81 suppliers
$86.00/250mg
234082-33-8
37 suppliers
$55.00/250mg
85474-75-5
81 suppliers
$86.00/250mg