4-TERT-BUTYL-PHENYL-HYDRAZINE synthesis
- Product Name:4-TERT-BUTYL-PHENYL-HYDRAZINE
- CAS Number:61765-93-3
- Molecular formula:C10H16N2
- Molecular Weight:164.25
3972-65-4
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Yield:-
Reaction Conditions:
Stage #1:1-bromo-4-tert-butylbenzene with t-butoxycarbonylhydrazine;t-BuBrettPhos;[tBuBrettPhosPd(allyl)]OTf;sodium t-butanolate in water at 45; for 1.5 h;Inert atmosphere;
Stage #2: with sulfuric acid in ethanol;water at 90 - 95;Inert atmosphere;Sealed tube;
References:
Akporji, Nnamdi;Braga, Felipe C.;Gabriel, Christopher M.;Landstrom, Evan B.;Lee, Nicholas R.;Lipshutz, Bruce H. [Organic Letters,2020] Location in patent:supporting information
3972-56-3
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7598-28-9
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$57.00/50mg
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769-92-6
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