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ChemicalBook CAS DataBase List 4-Vinylsulfonylbenzoic acid

4-Vinylsulfonylbenzoic acid synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: sodium hydroxide / water / 6 h / 20 - 40 °C
2: dihydrogen peroxide / acetic acid / 16 h / 20 °C / Darkness
3: methanesulfonyl chloride; triethylamine / dichloromethane / 16 h / 0 - 20 °C

References:

Kim, Junyong;Li, Beryl X.;Huang, Richard Y.-C.;Qiao, Jennifer X.;Ewing, William R.;Macmillan, David W. C. [Journal of the American Chemical Society,2020,vol. 142,# 51,p. 21260 - 21266]

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