Sulfoxonium, dimethyl-, (3S)-3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-oxo-4-phenylbutylide synthesis
- Product Name:Sulfoxonium, dimethyl-, (3S)-3-[[(1,1-dimethylethoxy)carbonyl]amino]-2-oxo-4-phenylbutylide
- CAS Number:400611-25-8
- Molecular formula:C17H25NO4S
- Molecular Weight:339.453
Yield:-
Reaction Conditions:
Stage #1: trimethylsulfoxonium iodidewith potassium tert-butylate in tetrahydrofuran; for 2 h;Heating;
Stage #2: N-t-butoxycarbonyl-L-phenylalanine 4-nitrophenyl ester in tetrahydrofuran at 0; for 4 h;
References:
Wang, Dengjin;Schwinden, Mark D.;Radesca, Lilian;Patel, Bharat;Kronenthal, David;Huang, Ming-Hsing;Nugent, William A. [Journal of Organic Chemistry,2004,vol. 69,# 5,p. 1629 - 1633]
13734-34-4
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