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ChemicalBook CAS DataBase List 1-Cyclopentene-1-heptanoic acid,5-oxo-3-[(tetrahydro-2H-pyran-2-yl)oxy]-, Methyl ester

1-Cyclopentene-1-heptanoic acid,5-oxo-3-[(tetrahydro-2H-pyran-2-yl)oxy]-, Methyl ester synthesis

14synthesis methods
34546-57-1 Synthesis
methyl 5-oxocyclopent-1-ene-1-heptanoate

34546-57-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 100 percent / N-bromosuccinimide, 2,2-azadiisobutyronitrile / CCl4 / 5 h / Heating
2: 62 percent / H2O / dioxane / 2.5 h / Heating
3: 72 percent / conc. HCl / 4 h / Ambient temperature

References:

Holland;Ratemi;Contreras [Canadian Journal of Chemistry,1994,vol. 72,# 1,p. 1 - 5]

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