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46155-89-9

1,3-DiMethyl-1H-pyrrolo[3,2-d]pyriMidine-2,4(3H,5H)-dione synthesis

6synthesis methods
-

Yield:46155-89-9 52% ,99747-54-3 14%

Reaction Conditions:

Stage #1: allyltriphenylphosphonium bromidewith lithium hydride in butanone at 20;
Stage #2: 6-azido-1,3-dimethylpyrimidine-2,4(1H,3H)-dione for 2 h;Heating;

References:

Abdou, Wafaa M.;Fahmy, Amin F. M.;Kamel, Azza A. [Heteroatom Chemistry,2002,vol. 13,# 4,p. 357 - 365]