Benzoic acid, 4-(4-carboxybenzoyl)-, 1-methyl ester synthesis

2synthesis methods

1679-64-7 Synthesis

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: SOCl₂
1.2: AlCl₃ / 25 °C
2.1: 74 percent / H₂SO₄; CrO₃ / acetic acid / 5 - 20 °C

References:

Salem, Ola I. A.;Schulz, Tobias;Hartmann, Rolf W. [Archiv der Pharmazie,2002,vol. 335,# 2-3,p. 83 - 88]

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