4H,5H,6H,7H,8H-thieno[3,2-c]azepin-4-one synthesis
- Product Name:4H,5H,6H,7H,8H-thieno[3,2-c]azepin-4-one
- CAS Number:4751-59-1
- Molecular formula:C8H9NOS
- Molecular Weight:167.23
13414-95-4
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$25.00/1g
4751-59-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 95 percent / hydroxylammonium chloride, pyridine / 2 h / Ambient temperature
2: 60 percent / phosphorus pentoxide, methanesulfonic acid / 5 h / 100 - 110 °C
References:
Cho, Hidetsura;Murakami, Kengo;Nakanishi, Hiroyuki;Isoshima, Hirotaka;Hayakawa, Kazuhide;Uchida, Itsuo [Heterocycles,1998,vol. 48,# 5,p. 919 - 927]
859204-24-3
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4751-59-1
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4651-81-4
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$7.00/1g
4751-59-1
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24287-95-4
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$7.00/100mg
4751-59-1
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76360-43-5
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$33.00/250mg
4751-59-1
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