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4H-Pyrrolo[2,3-d]thiazole synthesis

1synthesis methods
Carbamic acid, N-[5-[2-(triethylsilyl)ethynyl]-4-thiazolyl]-, 1,1-dimethylethyl ester

1258934-74-5
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4H-Pyrrolo[2,3-d]thiazole

298699-45-3
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Yield:298699-45-3 44%

Reaction Conditions:

with potassium tert-butylate in 1-methyl-pyrrolidin-2-one at 90; for 0.166667 h;Microwave irradiation;Inert atmosphere;sealed tube;

References:

Koolman, Hannes;Heinrich, Timo;Reggelin, Michael [Synthesis,2010,# 18,p. 3152 - 3162] Location in patent:experimental part