5-(3-fluorophenyl)pyridine-3,4-diamine synthesis
- Product Name:5-(3-fluorophenyl)pyridine-3,4-diamine
- CAS Number:1214358-61-8
- Molecular formula:C11H10FN3
- Molecular Weight:203.22
1681-37-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: anhydrous Sodium acetate; acetic acid; bromine / 110 °C
2: anhydrous sodium carbonate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II) / 1,4-dioxane; water monomer / 95 °C / Inert atmosphere
3: palladium on activated charcoal; hydrogen / methanol / 20 °C
References:
WO2022/12058,2022,A1
89284-05-9
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