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5,5-Dichloro-2,2'-Biphenyldiol synthesis

9synthesis methods
71643-66-8 Synthesis
4-Chloro-2-iodophenol

71643-66-8
135 suppliers
$6.00/250mg

5,5-Dichloro-2,2'-Biphenyldiol

31113-52-7
2 suppliers
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Yield:31113-52-7 80%

Reaction Conditions:

with [2,2]bipyridinyl;manganese powder;nickel(II) chloride ethylene glycol dimethyl ether complex;potassium-t-butoxide in N,N-dimethyl-formamide at 75; for 36 h;Sealed tube;Glovebox;Inert atmosphere;chemoselective reaction;

References:

Long, Cheng-Yu;Chen, Hao;Ma, Cheng;Zhao, Bo-Wei;Li, Shen-Huan;Cui, Yue;Yang, Xinge;Ni, Shao-Fei;Wang, Xue-Qiang [Organic Letters,2022,vol. 24,# 23,p. 4155 - 4159] Location in patent:supporting information