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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

5,5-dimethyl-2-(3-nitrophenyl)-1,3-dioxane synthesis

2synthesis methods
99-61-6 Synthesis
3-Nitrobenzaldehyde

99-61-6
633 suppliers
$5.00/10g

126-30-7 Synthesis
2,2-Dimethyl-1,3-propanediol

126-30-7
607 suppliers
$8.00/100g

5,5-dimethyl-2-(3-nitrophenyl)-1,3-dioxane

23281-36-9
4 suppliers
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Yield:23281-36-9 95%

Reaction Conditions:

with toluene-4-sulfonic acid in toluene at 140; for 24 h;Inert atmosphere;

References:

Robertson, Linsey;Hartley, Richard C. [Tetrahedron,2009,vol. 65,# 27,p. 5284 - 5292] Location in patent:experimental part

1,5,7,11-Tetraoxaspiro[5.5]undecane, 3,3,9,9-tetramethyl-

65849-85-6
0 suppliers
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99-61-6 Synthesis
3-Nitrobenzaldehyde

99-61-6
633 suppliers
$5.00/10g

3592-12-9 Synthesis
5,5-DIMETHYL-1,3-DIOXAN-2-ONE

3592-12-9
35 suppliers
$34.43/1g

5,5-dimethyl-2-(3-nitrophenyl)-1,3-dioxane

23281-36-9
4 suppliers
inquiry

References