(5-BroMopyridin-3-yl)(phenyl)Methanone synthesis
- Product Name:(5-BroMopyridin-3-yl)(phenyl)Methanone
- CAS Number:59105-50-9
- Molecular formula:C12H8BrNO
- Molecular Weight:262.1
233770-01-9
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135364-97-5
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59105-50-9
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Yield:59105-50-9 62%
Reaction Conditions:
Stage #1: 3-bromo-5-iodopyridinewith TurboGrignard in tetrahydrofuran at -20; for 0.833333 h;Inert atmosphere;Schlenk technique;
Stage #2: tert-butyl benzoyl(tert-butoxycarbonyl)carbamate in tetrahydrofuran at -20 - 20; for 2.5 h;Inert atmosphere;Schlenk technique;chemoselective reaction;
References:
Li, Guangchen;Szostak, Michal [Chemistry - A European Journal,2020,vol. 26,# 3,p. 611 - 615] Location in patent:supporting information
100-58-3
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183608-47-1
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591-51-5
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$123.00/50ml
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233770-01-9
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$8.00/250mg
6919-61-5
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59105-50-9
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