(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE synthesis
- Product Name:(5''-CHLORO-2'',3''-DIMETHOXY)ACETOPHENONE
- CAS Number:117052-19-4
- Molecular formula:C10H11ClO3
- Molecular Weight:214.65
117052-18-3
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117052-19-4
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Yield:117052-19-4 96%
Reaction Conditions:
with manganese(IV) oxide in chloroform; for 8 h;Reflux;
Steps:
5
Example 5; The synthesis of ketone 3 was carried out by reducting the commercially available aldehyde 1 to the corresponding alcohol 2 following the procedure disclosed in WO06/081332A1, followed by the oxidation to ketone 3 with MnO2 with a good yield (Scheme 8).
References:
EP2103596,2009,A1 Location in patent:Page/Page column 50
86232-28-2
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117052-19-4
18 suppliers
$90.00/50mg