ChemicalBook CAS DataBase List 5-hexylbenzene-1,3-diol

5-hexylbenzene-1,3-diol synthesis

8synthesis methods

Product Name:5-hexylbenzene-1,3-diol
CAS Number:5465-20-3
Molecular formula:C12H18O2
Molecular Weight:194.27

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux
2: hydrogen, conc. H₂SO₄ / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature
3: NaI, ClSiMe₃ / acetonitrile / 36 h / Heating

References:

Ayer, William A.;Browne, Lois M.;Lovell, Sarah H. [Phytochemistry,1983,vol. 22,# 10,p. 2267 - 2272]

1132-21-4 Synthesis