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ChemicalBook CAS DataBase List 5-HYDROXY-HEXAHYDRO-CYCLOPENTA[B]FURAN-2-ONE
84173-27-3

5-HYDROXY-HEXAHYDRO-CYCLOPENTA[B]FURAN-2-ONE synthesis

3synthesis methods
2H-Cyclopenta[b]furan-2-one, 4-bromohexahydro-5-hydroxy-, (3aS,4R,5R,6aS)-

132747-01-4
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Yield:84173-27-3 92%

Reaction Conditions:

with tri-n-butyl-tin hydride;2,2'-azobis(isobutyronitrile) in benzene; for 24 h;Heating;

References:

Corey;Carpino, Philip [Tetrahedron Letters,1990,vol. 31,# 52,p. 7555 - 7558]