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864756-01-4

5-Iodo-3-methoxy-7-methylbenzo[d]isoxazole synthesis

4synthesis methods
Benzamide, N,2-dihydroxy-5-iodo-3-methyl-

864755-98-6
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5-Iodo-3-methoxy-7-methylbenzo[d]isoxazole

864756-01-4
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 99 percent / carbonyldiimidazole / tetrahydrofuran / 2 h / Heating
2: 38 percent / potassium carbonate / dimethylsulfoxide / 24 h / 20 °C

References:

Deng, Bo-Liang;Hartman, Tracy L.;Buckheit Jr., Robert W.;Pannecouque, Christophe;De Clercq, Erik;Fanwick, Phillip E.;Cushman, Mark [Journal of Medicinal Chemistry,2005,vol. 48,# 19,p. 6140 - 6155]