5-Iodo-pyrimidine-2,4-diamine synthesis
- Product Name:5-Iodo-pyrimidine-2,4-diamine
- CAS Number:157924-46-4
- Molecular formula:C4H5IN4
- Molecular Weight:236.01
156-81-0
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Yield:157924-46-4 97%
Reaction Conditions:
Stage #1: pyrimidine-2,4-diaminewith periodic acid;sulfuric acid;iodine;acetic acid in water monomer; for 5.5 h;
Stage #2: with potassium hydroxide in water monomer at 20;
References:
Wellington, Kevin W.;Ooi, Hua Chee;Benner, Steven A. [Nucleosides, nucleotides and nucleic acids,2009,vol. 28,# 4,p. 275 - 291] Location in patent:experimental part