5-METHOXY-1H-INDOLE-2-BORONIC ACID PINACOL ESTER synthesis
- Product Name:5-METHOXY-1H-INDOLE-2-BORONIC ACID PINACOL ESTER
- CAS Number:683229-62-1
- Molecular formula:C15H20BNO3
- Molecular Weight:273.14
1006-94-6
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$10.00/5g
73183-34-3
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$6.00/5g
683229-62-1
28 suppliers
$45.00/25mg
Yield:683229-62-1 83%
Reaction Conditions:
Stage #1: bis(pinacol)diboranewith 5-methyl-2-(thiophen-3-yl)pyridine;(1,5-cyclooctadiene)(methoxy)iridium(I) dimer in tetrahydrofuran at 20; for 0.0333333 h;Inert atmosphere;Glovebox;
Stage #2: 5-methoxylindole in tetrahydrofuran at 80; for 12 h;Inert atmosphere;Sealed tube;regioselective reaction;
References:
Chattopadhyay, Buddhadeb;Hassan, Mirja Md Mahamudul;Hoque, Md Emdadul [Journal of the American Chemical Society,2021,vol. 143,# 13,p. 5022 - 5037] Location in patent:supporting information
1006-94-6
507 suppliers
$10.00/5g
25015-63-8
224 suppliers
$22.39/5G
683229-62-1
28 suppliers
$45.00/25mg