(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID synthesis
- Product Name:(5-METHOXY-2-NITRO-PHENYL)-ACETIC ACID
- CAS Number:20876-29-3
- Molecular formula:C9H9NO5
- Molecular Weight:211.17
89302-15-8
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20876-29-3
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Yield:20876-29-3 87%
Reaction Conditions:
with hydrogenchloride;acetic acid for 4 h;Reflux;
Steps:
Typical procedure for the hydrolysis of the nitrileunder acid conditions:
General procedure: 1 equivalent of nitrile was dissolved in a mixture of AcOH/HCl (1:5) andrefluxed for 4 h. The product was extracted with ethyl acetate, dried over Na2SO4and evaporated.
References:
Schlosser, Joachim;Johannes, Eugen;Zindler, Melanie;Lemmerhirt, Jan;Sommer, Benjamin;Schütt, Martin;Peifer, Christian [Tetrahedron Letters,2015,vol. 56,# 1,p. 89 - 94] Location in patent:supporting information
117559-88-3
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20876-29-3
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5367-32-8
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$10.00/5g
95-92-1
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$5.00/5G
20876-29-3
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$39.00/100mg
2581-34-2
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20876-29-3
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$39.00/100mg
100-17-4
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$23.00/25g
20876-29-3
60 suppliers
$39.00/100mg