(5-METHYL-1-BENZOTHIEN-3-YL)ACETONITRILE synthesis
1synthesis methods
- Product Name:(5-METHYL-1-BENZOTHIEN-3-YL)ACETONITRILE
- CAS Number:23799-59-9
- Molecular formula:C11H9NS
- Molecular Weight:187.26
Yield:23799-59-9 46%
Reaction Conditions:
with potassium phosphate;[nickel(II)dichloride(dimethoxyethane)];[4,4'-bis(1,1-dimethylethyl)-2,2'-bipyridine-N1,N1]bis-{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C}iridium(III) hexafluorophosphate;4,4'-di-tert-butyl-2,2'-bipyridine at 20; for 72 h;Irradiation;Sealed tube;
References:
Kariofillis, Stavros K.;Shields, Benjamin J.;Tekle-Smith, Makeda A.;Zacuto, Michael J.;Doyle, Abigail G. [Journal of the American Chemical Society,2020,vol. 142,# 16,p. 7683 - 7689] Location in patent:supporting information