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ChemicalBook CAS DataBase List 5-methyl-1H-pyrrole-2-carbonitrile(SALTDATA: FREE)

5-methyl-1H-pyrrole-2-carbonitrile(SALTDATA: FREE) synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; sodium acetate / methanol / 0.5 h / 20 °C
2: 1,1'-carbonyldiimidazole / chloroform / 16 h / 20 °C / Inert atmosphere

References:

Damke, Jan-Erik;Koenig, Torben;Haake, Gerold;Latos-Grazynski, Lechoslaw;Monltorls, Franz-Peter [Heterocycles,2011,vol. 82,# 2,p. 1503 - 1514]