5-Tetradecyn-1-ol synthesis
- Product Name:5-Tetradecyn-1-ol
- CAS Number:25593-82-2
- Molecular formula:C14H26O
- Molecular Weight:210.36
Yield:25593-82-2 62%
Reaction Conditions:
Stage #1: 5-hexyl-1-olwith n-butyllithium in tetrahydrofuran;N,N,N,N,N,N-hexamethylphosphoric triamide at -10 - 20; for 3 h;
Stage #2: 1-Iodooctane in tetrahydrofuran;N,N,N,N,N,N-hexamethylphosphoric triamide;
References:
Verniest, Guido;Boterberg, Stefaan;Colpaert, Jeroen;Van Thienen, Tinneke;Stevens, Christian V.;De Kimpe, Norbert [Synlett,2004,# 7,p. 1273 - 1275]
1720-37-2
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$160.00/500mg
111-83-1
503 suppliers
$12.00/25g
25593-82-2
9 suppliers
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