Dimethyl 5,6,7,8-tetrahydronaphthalene-2,3-dicarboxylate synthesis
- Product Name:Dimethyl 5,6,7,8-tetrahydronaphthalene-2,3-dicarboxylate
- CAS Number:51510-78-2
- Molecular formula:C14H16O4
- Molecular Weight:248.27
108-94-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: phosphorus tribromide / dichloromethane / 2 h / 0 °C / Inert atmosphere
1.2: 20 h / 0 - 20 °C / Inert atmosphere
1.3: pH Ca. 7 / Inert atmosphere; Cooling with ice
2.1: palladium diacetate; triphenylphosphine; sodium acetate / tetrahydrofuran / 20 h / 125 °C / Inert atmosphere
References:
Li, Renlong;Liu, Gongchu;Xie, Ruihao;Wang, Zhenfeng;Yang, Xiye;An, Kang;Zhong, Wenkai;Jiang, Xiao-Fang;Ying, Lei;Huang, Fei;Cao, Yong [Journal of Materials Chemistry C,2018,vol. 6,# 26,p. 7046 - 7053]
