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5-Hydroxy-2-(4-methoxyphenyl)-3,7,8-trimethoxy-4H-1-benzopyran-4-one synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium carbonate; acetone
2: pyridine; aqueous KOH-solution; potassium peroxo disulfate / Erwaermen des Reaktionsprodukts mit wss. Salzsaeure und Natriumsulfit
3: diethyl ether; methanol; boric acid

References:

Brown et al. [Australian Journal of Chemistry,1954,vol. 7,p. 181,187]