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6,6-DIMETHYL-N~2~-PHENYL-1,6-DIHYDRO-1,3,5-TRIAZINE-2,4-DIAMINE synthesis

3synthesis methods
-

Yield:5405-66-3 1.86 g

Reaction Conditions:

with sodium hydroxide in ethanol;water; pH=11; for 1 h;Reflux;Dimroth rearrangement;

References:

Ma, Xiang;Poon, Thong-Yuen;Wong, Peter Tsun Hon;Chui, Wai-Keung [Bioorganic and Medicinal Chemistry Letters,2009,vol. 19,# 19,p. 5644 - 5647] Location in patent:supporting information; experimental part