6-Methyl-4-(trifluoromethyl)-2,3-dihydropyridazin-3-one synthesis

3synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 75 percent / PTSA; N₂H₄ / toluene / 5 h / Heating
2: 81 percent / CuCl₂ / acetonitrile / 7 h / Heating

References:

Brule, Cedric;Bouillon, Jean-Philippe;Nicolai, Eric;Portella, Charles [Synthesis,2003,# 3,p. 436 - 442]

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