5H-Benzo[b]phosphindole, 5-phenyl-, 5-oxide synthesis
- Product Name:5H-Benzo[b]phosphindole, 5-phenyl-, 5-oxide
- CAS Number:1031-13-6
- Molecular formula:C18H13OP
- Molecular Weight:276.269
84783-64-2
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$26.00/100mg
1031-13-6
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Yield:1031-13-6 99%
Reaction Conditions:
Stage #1: 2,2'-bis(diphenylphosphino)biphenylwith bis(1,5-cyclooctadiene)nickel (0);Phenyl triflate in N,N-dimethyl-formamide at 140; for 20 h;Glovebox;Inert atmosphere;Sealed tube;
Stage #2: with dihydrogen peroxide in water;N,N-dimethyl-formamide at 20; for 1 h;Glovebox;Inert atmosphere;Sealed tube;
References:
Fujimoto, Hayato;Kusano, Momoka;Kodama, Takuya;Tobisu, Mamoru [Organic Letters,2019,vol. 21,# 11,p. 4177 - 4181] Location in patent:supporting information
594-19-4
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$27.50/50ml
791-28-6
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$6.00/25g
1031-13-6
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![[tert-butyl(phenyl)phosphoryl]benzene](/CAS/20180601/GIF/56598-35-7.gif)
56598-35-7
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