6-(2,2,2-Trifluoro-ethoxy)-pyridin-3-ol synthesis
- Product Name:6-(2,2,2-Trifluoro-ethoxy)-pyridin-3-ol
- CAS Number:796120-81-5
- Molecular formula:C7H6F3NO2
- Molecular Weight:193.12
766-11-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium tert-butylate / tert-butyl methyl ether / 6 h / 0 - 20 °C
2: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 95 °C / Inert atmosphere
3: sodium perborate tetrahydrate / tetrahydrofuran; water / 4 h / 0 - 20 °C
References:
US2018/237419,2018,A1