6-Benzothiazolethiol,2-methyl-(9CI) synthesis

1synthesis methods

Yield:-

Steps:

Multi-step reaction with 3 steps
2: 76 percent / Pd(PPh₃)4 / tetrahydrofuran; benzene / 4 h / Heating
3: 72 percent / TBAF / tetrahydrofuran / 0 °C

References:

Arnould, Jean Claude;Didelot, Myriam;Cadilhac, Caroline;Pasquet, Marie Jeanne [Tetrahedron Letters,1996,vol. 37,# 26,p. 4523 - 4524]

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