6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL synthesis
- Product Name:6-BROMO-2,3-DIHYDRO-1H-INDEN-1-OL
- CAS Number:75476-86-7
- Molecular formula:C9H9BrO
- Molecular Weight:213.07
14548-39-1
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$10.00/1g
75476-86-7
67 suppliers
$20.00/250mg
Yield: 100%
Reaction Conditions:
with sodium tetrahydroborate in ethanol at 10 - 20; for 3 h;
Steps:
4 liquid crystal compound 3RIGUQUF
168.8g compd. 6 and 650 ml of ethanol is added during the reaction of the bottle. Next, the water temperature is lower than 10 °C, NaBH445g of small amounts of added. Next, raised in temperature to room temperature, the reaction solution is a 3-hour continuous agitation. After the reaction is completed, ethanol is removed, then the hydrolysis of 10% HCl 450 ml is added is in order. The mixture is extracted by dichlomethane, thereafter is washed with water, dried and then, the solvent is removed, 170g compd. 7 in which yield 100% (corallite solid). The reaction of the pathway of the following relationships.
References:
DAXIN MATERIALS CORPORATION;LEE, CHING-TIEN;LIU, HSIN-CHENG;WANG, CHUN-CHIH;JIANG, TIAN-MENG;TIAN, HUI-QUIANG;GAO, LI-LONG;HUANG, WAN-YU JP2016/29040, 2016, A Location in patent:Paragraph 0058
1643-30-7
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$6.00/1g
75476-86-7
67 suppliers
$20.00/250mg
55394-81-5
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inquiry
75476-86-7
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70146-78-0
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$28.00/100mg
75476-86-7
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$20.00/250mg
92013-18-8
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$147.00/500mg
75476-86-7
67 suppliers
$20.00/250mg