6-broMo-N-Methyl-1,3-benzothiazol-2-aMine synthesis
- Product Name:6-broMo-N-Methyl-1,3-benzothiazol-2-aMine
- CAS Number:75104-92-6
- Molecular formula:C8H7BrN2S
- Molecular Weight:243.12
80945-86-4
202 suppliers
$8.00/1g
74-89-5
0 suppliers
$13.44/25ML
75104-92-6
33 suppliers
$18.00/250mg
Yield:75104-92-6 87.9%
Reaction Conditions:
at 60;Sealed tube;
Steps:
5
[00394]6-Bromo-2-chlorobenzo[d]thiazole (701) (0.5 g, 2.0 mmol) was dissolved in methanamine solution (20 ml) in a sealed tube, and the resulting mixture was stirred at 60° C. overnight. The mixture was allowed to cool to RT, concentrated in vacuo and water (20 mL) was added. The solid was collected by filtration to afford the desired product, 6-bromo-N-methylbenzo[d]thiazol-2-amine (702) (0.43 g, 87.9% yield). ESI-MS (M+H)+m/z: 242.8.
References:
US2015/225407,2015,A1 Location in patent:Paragraph 0416
15864-32-1
234 suppliers
$6.00/1g
74-89-5
0 suppliers
$13.44/25ML
75104-92-6
33 suppliers
$18.00/250mg
61449-55-6
23 suppliers
inquiry
75104-92-6
33 suppliers
$18.00/250mg
2724-69-8
81 suppliers
$22.00/1g
75104-92-6
33 suppliers
$18.00/250mg
106-40-1
491 suppliers
$12.00/5g
75104-92-6
33 suppliers
$18.00/250mg