6-CHLORO-2,3-DIHYDRO-2,2-DIMETHYL-1H-INDEN-1-ONE synthesis

1synthesis methods

Product Name:6-CHLORO-2,3-DIHYDRO-2,2-DIMETHYL-1H-INDEN-1-ONE
CAS Number:13099-73-5
Molecular formula:C11H11ClO
Molecular Weight:194.66

14548-38-0
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74-88-4
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6-CHLORO-2,3-DIHYDRO-2,2-DIMETHYL-1H-INDEN-1-ONE

13099-73-5
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Yield:13099-73-5 95%

Reaction Conditions:

Stage #1: 6-chloro-1-indanonewith sodium hydride in tetrahydrofuran;mineral oil at 0; for 0.5 h;Inert atmosphere;
Stage #2: methyl iodide in tetrahydrofuran;mineral oil at 0 - 20;Inert atmosphere;

References:

Chen, Jun;Shi, Zhan;Lu, Ping [Organic Letters,2021,vol. 23,# 19,p. 7359 - 7363] Location in patent:supporting information

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