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ChemicalBook CAS DataBase List 6-IODO-2-METHYL-1,3-BENZOTHIAZOLE 90
68867-20-9

6-IODO-2-METHYL-1,3-BENZOTHIAZOLE 90 synthesis

9synthesis methods
-

Yield:68867-20-9 79%

Reaction Conditions:

Stage #1: 6-amino-2-methylbenzothiazolewith hydrogenchloride;sodium nitrite for 0.5 h;cooling;
Stage #2: with potassium iodide in water at 40; for 0.166667 h;

References:

Santos, Paulo F.;Reis, Lucinda V.;Duarte, Isabel;Serrano, Joao P.;Almeida, Paulo;Oliveira, Anabela S.;Ferreira, Luis F. Vieira [Helvetica Chimica Acta,2005,vol. 88,# 5,p. 1135 - 1143]