6-Methoxy-3-Methylisoquinolin-1(2H)-one synthesis
- Product Name:6-Methoxy-3-Methylisoquinolin-1(2H)-one
- CAS Number:869897-98-3
- Molecular formula:C11H11NO2
- Molecular Weight:189.21
918662-40-5
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Yield:869897-98-3 270 mg (74%)
Reaction Conditions:
in ammonium hydroxide;
Steps:
15.2 Step 2
Step 2 6-Methoxy-3-methylisoquinolin-1(2H)-one. The cyclic anhydride of step 1 (405 mg; 1.73 mmol) was dissolved in aqueous ammonium hydroxide, and heated at reflux for 1.5 hours. The mixture was cooled to room temperature and the solid was filtered then dried overnight to give 270 mg (74%) of 6-methoxy-3-methylisoquinolin-1(2H)-one.
References:
US2009/203629,2009,A1
71568-84-8
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869897-98-3
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6245-57-4
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68294-03-1
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$310.00/500mg
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