(6-methoxynaphthalen-2-yl)methanamine synthesis

2synthesis methods

Product Name:(6-methoxynaphthalen-2-yl)methanamine
CAS Number:177736-15-1
Molecular formula:C12H13NO
Molecular Weight:187.24

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Yield:177736-15-1 90%

Steps:

31 31A 2-Aminomethyl-6-methoxynaphthalene

31A 2-Aminomethyl-6-methoxynaphthalene Following the process described in example 1 (point E), starting from 2-cyano-6-methoxynaphthalene, the title compound was prepared (90% yield). ¹H N.M.R. (300 MHz, CD₃OD) δ ppm: 3.92 (s, 3H); 4.25 (s, 2H); 7.19 (dd, 1H); 7.28 (d, 1H); 7.50 (dd, 1H); 7.79-7.88 (m, 3H).

References:

EP775133,2001,B1

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References