6-methyl-6-hepten-2-one synthesis
- Product Name:6-methyl-6-hepten-2-one
- CAS Number:10408-15-8
- Molecular formula:C8H14O
- Molecular Weight:126.2
624-45-3
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Yield:-
Steps:
Multi-step reaction with 8 steps
1: 1.) p-CH3C6H4SO3H, 2.) LAH / 1.) C6H6
2: 86 percent / pyridinium chlorochromate, sodium acetate / CH2Cl2 / 0.75 h / 25 °C
3: 1.) sodium hydride / 1.) ether, 25 deg C, 45 min, 2.) 3 h
4: 98 percent / hydrogen / 5percent Pd-C / methanol / 12 h / 25 °C
5: 93 percent / lithium aluminum hydride / diethyl ether / 2 h / 0 °C
6: 86 percent / hydrochloric acid / diethyl ether / 3 h / 25 °C
7: 97 percent / pyridine
8: 1.) sodium iodide, 2.) DBU / 1.) DMF, 50 deg C, 3.5 h, 2.) 80 deg C, 3.5 h
References:
Dhokte, U. P.;Rao, A. S. [Synthetic Communications,1988,vol. 18,# 8,p. 811 - 822]
17123-64-7
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