ChemicalBook CAS DataBase List 6-PHENYL-1-HEXANOL

6-PHENYL-1-HEXANOL synthesis

10synthesis methods

Product Name:6-PHENYL-1-HEXANOL
CAS Number:2430-16-2
Molecular formula:C12H18O
Molecular Weight:178.27

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Yield: 70%

Reaction Conditions:

with hydrogen;palladium on activated charcoal in ethanol under 2068.65 Torr; for 2 h;

Steps:

General Method for hydrogen ation of alkyneThe desired alkyne is dissolved in ethanol and a heterogeneous mixture of ^' palladium on carbon is added. The reaction is shaken for 2 hours under 40 psi of H₂. Filtration through celite and removal of the solvent in vacuo gives the desired product.; 6-Phenylhexan-l-olThe title compound was prepared from 6-phenylhex-5-yn-l-ol in 70 % (241 mg) yield. ¹H NMR (400 MHz, CDCl₃) δ 7.18-7.27 (m, 2H), 7.16-7.18 (m, 3H) 3.63 (t, 2H, J = 6.4 Hz), 2.61 (t, 2H₅ J= 8.0 Hz), 1.56-1.69 (m, 4H)₅ 1.37-1.40 (m, 5H).

References:

Location in patent:Page/Page column 89-90

5581-75-9 Synthesis