(4-hydroxy-7,7-dimethyl-2,6,8-trioxabicyclo[3.3.0]oct-3-yl)methyl benz oate synthesis

7synthesis methods

Product Name:(4-hydroxy-7,7-dimethyl-2,6,8-trioxabicyclo[3.3.0]oct-3-yl)methyl benz oate
CAS Number:6022-96-4
Molecular formula:C15H18O6
Molecular Weight:294.3

769-78-8 Synthesis

769-78-8
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1,2-O-Isopropylidene-alpha-D-xylofuranose

20031-21-4
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(4-hydroxy-7,7-dimethyl-2,6,8-trioxabicyclo[3.3.0]oct-3-yl)methyl benz oate

6022-96-4
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Yield:6022-96-4 96%

Reaction Conditions:

with Candida antarctica lipase B immobilized on polyacrylate in tetrahydrofuran at 40; for 1.16667 h;regioselective reaction;Reagent/catalyst;Solvent;

References:

Arya, Anu;Mathur, Divya;Tyagi, Abhilash;Kumar, Rajesh;Kumar, Vinod;Olsen, Carl E.;Saxena, Rajendra K.;Prasad, Ashok K. [Nucleosides, nucleotides and nucleic acids,2013,vol. 32,# 12,p. 646 - 659]

98-88-4 Synthesis