alpha-((MethylaMino)Methyl)benzeneMethanol hydrochloride synthesis
- Product Name:alpha-((MethylaMino)Methyl)benzeneMethanol hydrochloride
- CAS Number:6027-95-8
- Molecular formula:C9H14ClNO
- Molecular Weight:187.6666
68579-60-2
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Yield:6027-95-8 95%
Reaction Conditions:
with hydrogenchloride in ethyl acetate at 3; pH=1; for 1.5 h;Solvent;Temperature;
Steps:
7 Example 7
The reaction residue synthesized in Example 3 was dissolved in 100 mL of ethyl acetate.Pass hydrogen chloride gas to saturation,Adjust the solution pH to 1,To a large number of white solids precipitated, after stirring for 1.5 hours at 3 °C,After the solid was rinsed once with cooled 100 mL ethyl acetate,Dried at 65°C to give 254 g of N-methylphenylethanolamine hydrochloride,Yield 95%, purity 99.1%.
References:
CN106831453,2017,A Location in patent:Paragraph 0039; 0057-0064
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100-42-5
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$20.00/25mL
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