(Z)-Methyl 2-(tert-butoxycarbonylaMino)but-2-enoate synthesis

2synthesis methods

Product Name:(Z)-Methyl 2-(tert-butoxycarbonylaMino)but-2-enoate
CAS Number:63658-16-2
Molecular formula:C10H17NO4
Molecular Weight:215.25

56776-41-1 Synthesis

2-Butenoic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, methyl ester, (2E)-

56776-41-1
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(Z)-Methyl 2-(tert-butoxycarbonylaMino)but-2-enoate

63658-16-2
42 suppliers
$29.00/250mg

Yield:63658-16-2 90%

Reaction Conditions:

with iodine in tetrahydrofuran at 20; for 19 h;Inert atmosphere;optical yield given as %de;

References:

Kometani, Miki;Ihara, Kohki;Kimura, Rumi;Kinoshita, Hideki [Bulletin of the Chemical Society of Japan,2009,vol. 82,# 3,p. 364 - 380] Location in patent:experimental part

(+/-)-BOC-ALPHA-PHOSPHONOGLYCINE TRIMETHYL ESTER

121056-95-9
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75-07-0 Synthesis

75-07-0
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$14.00/5mL

63658-16-2
42 suppliers
$29.00/250mg

References

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