Acetamide, N-[2-hydroxy-3-[4-[[2-(1-methylethoxy)ethoxy]methyl]phenoxy]propyl]-N-(1-methylethyl)- synthesis
- Product Name:Acetamide, N-[2-hydroxy-3-[4-[[2-(1-methylethoxy)ethoxy]methyl]phenoxy]propyl]-N-(1-methylethyl)-
- CAS Number:66722-65-4
- Molecular formula:C20H33NO5
- Molecular Weight:367.48
66722-65-4
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Yield:-
Steps:
89 EXAMPLE 89
EXAMPLE 89 10 g. of N-[2-hydroxy-3-(p-2-isopropoxyethoxymethylphenoxy)-propyl]-N-isopropyl-acetamide [obtainable by reacting Na p-(2-isopropoxyethoxymethyl)-phenolate with N-(2-hydroxy-3-bromo-propyl)-N-isopropyl-acetamide] were boiled for 4 hours with 250 ml. of 20% hydrochloride acid. The mixture was evaporated and worked up in the customary manner to give 1-(p-2-isopropoxyethoxymethyl-phenoxy)-3-isopropylamino-propan-2-ol, fumarate, m.p. 100°.
References:
US4171370,1979,A