1,3-Benzenedicarboxylic acid, 5-[Methyl(Methylsulfonyl)aMino]-,MonoMethyl ester synthesis
- Product Name:1,3-Benzenedicarboxylic acid, 5-[Methyl(Methylsulfonyl)aMino]-,MonoMethyl ester
- CAS Number:695215-94-2
- Molecular formula:C11H13NO6S
- Molecular Weight:287.29
99-27-4
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695215-94-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 95 percent / pyridine / CH2Cl2 / 14 h / 23 °C
2.1: NaH / dimethylformamide / 23 °C
2.2: 91 percent / dimethylformamide / 5 h / 23 °C
3.1: 82 percent / NaOH / tetrahydrofuran; methanol; H2O / 14 h / 23 °C
References:
Ghosh, Arun K.;Kumaragurubaran, Nagaswamy;Hong, Lin;Kulkarni, Sarang S.;Xu, Xiaoming;Chang, Wanpin;Weerasena, Vajira;Turner, Robert;Koelsch, Gerald;Bilcer, Geoffrey;Tang, Jordan [Journal of Medicinal Chemistry,2007,vol. 50,# 10,p. 2399 - 2407]
695215-93-1
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695215-94-2
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62814-45-3
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695215-94-2
14 suppliers
$56.00/100mg